Observing in-phase single-quantum 15N multiplets for NH2/NH3+ groups with two-dimensional heteronuclear correlation spectroscopy.
Takayama Y, Sahu D, Iwahara J.
Takayama Y, et al. Among authors: iwahara j.
J Magn Reson. 2008 Oct;194(2):313-6. doi: 10.1016/j.jmr.2008.07.018. Epub 2008 Jul 23.
J Magn Reson. 2008.
PMID: 18691921
Free PMC article.
Here, we present a 2D F1-(1)H-coupled (1)H-(15)N heteronuclear correlation experiment that provides a 1:3:3:1 quartet for AX(3) spin system and a 1:2:1 triplet for AX(2). The experiment is a derivative of 2D HISQC experiment [J. Iwahara, Y.S. Jung, G.M. Clore, Heter …
Here, we present a 2D F1-(1)H-coupled (1)H-(15)N heteronuclear correlation experiment that provides a 1:3:3:1 quartet for AX(3) spin system …