Assignment of the side-chain 1H and 13C resonances of interleukin-1 beta using double- and triple-resonance heteronuclear three-dimensional NMR spectroscopy.
Clore GM, Bax A, Driscoll PC, Wingfield PT, Gronenborn AM.
Clore GM, et al. Among authors: wingfield pt.
Biochemistry. 1990 Sep 4;29(35):8172-84. doi: 10.1021/bi00487a027.
Biochemistry. 1990.
PMID: 2261471
As the NH, 15N, and C alpha H chemical shifts had previously been sequentially assigned by 3D 1H Hartmann-Hahn 15N-1H multiple quantum coherence (3D HOHAHA-HMQC) and 3D heteronuclear 1H nuclear Overhauser 15N-1H multiple quantum coherence (3D NOESY-HMQC) spectroscopy [Driscoll, …
As the NH, 15N, and C alpha H chemical shifts had previously been sequentially assigned by 3D 1H Hartmann-Hahn 15N-1H multiple quantum coher …